Detection Oriented Derivatization Techniques In Liquid Chromatography

Author : Henk Lingeman
Publisher : CRC Press
ISBN 13 : 1000444627
Total Pages : 414 pages
Book Rating : 4.29/5 ( download)

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Download or read book Detection-Oriented Derivatization Techniques in Liquid Chromatography written by Henk Lingeman and published by CRC Press. This book was released on 2021-05-30 with total page 414 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book covers the principles, kinetics, and applications of derivatization reactions in liquid chromatography. It emphasizes detection-oriented derivatization procedures that can be used to enhance to detectability of a wide variety of solutes using absorbance and fluorescence detection.

Author : H. Lingeman
Publisher : CRC Press
ISBN 13 : 9780824782870
Total Pages : 432 pages
Book Rating : 4.79/5 ( download)

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Download or read book Detection-Oriented Derivatization Techniques in Liquid Chromatography written by H. Lingeman and published by CRC Press. This book was released on 1990-01-19 with total page 432 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Author : J.F. Lawrence
Publisher : Elsevier
ISBN 13 : 0080858074
Total Pages : 223 pages
Book Rating : 4.74/5 ( download)

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Download or read book Chemical Derivatization in Liquid Chromatography written by J.F. Lawrence and published by Elsevier. This book was released on 2000-04-01 with total page 223 pages. Available in PDF, EPUB and Kindle. Book excerpt: Chemical Derivatization in Liquid Chromatography

Author : C.F. Poole
Publisher : Elsevier Inc. Chapters
ISBN 13 : 0128071079
Total Pages : 53 pages
Book Rating : 4.76/5 ( download)

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Download or read book Liquid Chromatography written by C.F. Poole and published by Elsevier Inc. Chapters. This book was released on 2013-01-08 with total page 53 pages. Available in PDF, EPUB and Kindle. Book excerpt: Derivatization employs various microchemical reactions to alter the structure of the analyte to facilitate its isolation, separation or detection. Reactions are commonly performed either off-line and prior to the separation or on-line and after the separation and prior to detection. Reagents and reaction conditions are suggested for improved uv-visible detection, fluorescence and chemiluminescence detection, electrochemical detection, mass spectrometric detection, separation of enatiomers, formation of cyclic derivatives, and solid-phase analytical derivatization. The design of reactors for post-column reactions are described for continuous detection in an automated mode.

Author : R. W. Frei
Publisher : Springer Science & Business Media
ISBN 13 : 1461591945
Total Pages : 353 pages
Book Rating : 4.48/5 ( download)

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Download or read book Chemical Derivatization in Analytical Chemistry written by R. W. Frei and published by Springer Science & Business Media. This book was released on 2013-04-17 with total page 353 pages. Available in PDF, EPUB and Kindle. Book excerpt: The first volume in this series is devoted to derivatization techniques in chromatography, for very obvious reasons. In gas chromatography (GC) chemical derivatization as an aid to expand the usefulness of the technique has been known for more than a decade and has become an established approach. The first chapter deals to a great extent with derivatization for the purpose of making compounds amenable to Gc. Although the discussion concentrates on pesticides, some generally valid conclusions can be drawn from this chapter. Chemistry will not be limited to the separation-it can also have a pronounced impact on the sample cleanup, another topic cov ered in Chapter 1. Since the introduction of coupled GC-mass spectroscopy (GC-MS), a very powerful tool, derivatization techniques have taken still another di rection-taking into consideration chromatographic as well as mass spec trometric improvement of the compounds of interest. Cyclic boronates are discussed as derivatization reagents for this purpose in the second chapter.

Author : George Lunn
Publisher : Wiley-Interscience
ISBN 13 : 9780471238881
Total Pages : 1832 pages
Book Rating : 4.80/5 ( download)

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Download or read book Handbook of Derivatization Reactions for HPLC written by George Lunn and published by Wiley-Interscience. This book was released on 1998-08-25 with total page 1832 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thousands of derivatization procedures for HPLC and CE-an essential tool for today's analytical chemist. This valuable reference offers fast and convenient access to derivatization reactions for both HPLC and capillary electrophoresis (CE). Covering a wide variety of compounds from pharmaceutical drugs and biological products to industrial contaminants, it is organized first by functional group and then by individual reagents. Techniques for each functional group are described in sufficient detail that the researcher can replicate procedures without reference to the original publications-saving hours of tedious library research. And because detailed procedures for the same reagent are listed together, it is easy to combine features of different methods and tailor them to fit specific individual requirements. Also available on CD-ROM, Handbook of Derivatization Reactions for HPLC contains fully abstracted and evaluated procedures from more than 1,900 papers, with descriptions of hundreds of reagents. A further 3,000 papers are referenced in bibliographies that are clearly annotated to help analysts identify those sources likely to be most useful. This important new resource will be welcomed by chemists working in pharmaceutical, biomedical, and environmental analysis. Also available on CD-ROM System requirements . . . IBM-compatible PC 486 or better and Windows(r) 3.0 or higher, or Macintosh 68030 processor and System 7 or higher * CD-ROM drive and 8 MB RAM minimum * 5 MB free hard disk space minimum, 30 MB recommended for full installation.

Author : Danilo Corradini
Publisher : CRC Press
ISBN 13 : 1420016946
Total Pages : 715 pages
Book Rating : 4.49/5 ( download)

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Download or read book Handbook of HPLC written by Danilo Corradini and published by CRC Press. This book was released on 2016-04-19 with total page 715 pages. Available in PDF, EPUB and Kindle. Book excerpt: High performance liquid chromatography (HPLC) is one of the most widespread analytical and preparative scale separation techniques used for both scientific investigations and industrial and biomedical analysis. Now in its second edition, this revised and updated version of the Handbook of HPLC examines the new advances made in this field since the

Author : Chi-San Wu
Publisher : CRC Press
ISBN 13 : 9780203913321
Total Pages : 720 pages
Book Rating : 4.29/5 ( download)

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Download or read book Handbook Of Size Exclusion Chromatography And Related Techniques written by Chi-San Wu and published by CRC Press. This book was released on 2003-11-04 with total page 720 pages. Available in PDF, EPUB and Kindle. Book excerpt: Documenting critical advances in this rapidly evolving field, the Second Edition highlights the need for new applications and technologies that assist in the determination of molecular weight and molecular weight distributions of polymers in an accurate, efficient manner. This volume presents the latest findings from a international team of specialists and continues to inspire and extend practical applications of size exclusion chromatography (SEC). It includes six new chapters covering high-speed size exclusion chromatography, SEC of low molecular weight materials, and the extended family of techniques, from two-dimensional liquid chromatography to high osmotic pressure chromatography.

Author : Milos Krejci
Publisher : CRC Press
ISBN 13 : 1000147975
Total Pages : 224 pages
Book Rating : 4.71/5 ( download)

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Download or read book Trace Analysis with Microcolumn Liquid Chromatography written by Milos Krejci and published by CRC Press. This book was released on 2020-07-24 with total page 224 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book provides a detailed description of technical elements of a microbore column liquid chromatograph suitable for use in trace analysis. It presents examples of analyses, especially from the spheres of biochemistry, pharmacology, and environmental analytical chemistry.

Author : A. Townshend
Publisher : CRC Press
ISBN 13 : 0412351501
Total Pages : 1422 pages
Book Rating : 4.01/5 ( download)

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Download or read book Dictionary of Analytical Reagents written by A. Townshend and published by CRC Press. This book was released on 1993-06-17 with total page 1422 pages. Available in PDF, EPUB and Kindle. Book excerpt: This volume dictionary brings together accurate chemical, structural and bibliographic data on the most commonly used reagents in the various branches of analytical chemistry. Covering both organic and inorganic compounds, the "Dictionary of Analytical Reagents" contains over 5,000 reagents significant in analytical chemistry, grouped into 5,000 entries. All the reagents included in the dictionary have been synthesized, characterized by or are of proven use to analytical chemists. Compiled by a distinguished board of leading figures in the world of analytical chemistry, each an expert in their own specialist field, the "Dictionary of Analytical Reagents" is a companion volume to the renowned "Dictionary of Organic Compounds" and follows a similar format. The dictionary is arranged in such a way as to facilitate browsing, with entries ordered alphabetically by entry name (often its trivial name). Clearly laid out in an easy-to-follow manner, each entry contains a wealth of data invaluable to the analytical chemist including synonyms, analytical applications, extensive and up-to-date hazard/toxicity data, solubility, dissociation constant and selected references labelled to indicate their content (e.g. analytical application, spectral data, synthesis). High quality structure diagrams are included to assist the analytical chemist in identifying the reagent needed and are drawn to standard orientations. Coverage extends to metal extractants, spectrophotometric reagents, indicators, fluorescence labelling reagents, resolving agents, nmr shift reagents and reference standards, buffers, gc and ms derivatisation reagents, amperometric reagents, titrimetric and gravimetric reagents, biological stains and dyes. Compounds are comprehensively indexed by Name, Molecular Formula, CAS Registry Number and Type of Compound. The unique Type of Compound Index is particularly valuable as compounds are indexed by use (eg NMR shift reagent), by analyte (eg nickel) and by compound group (eg formazan, crown ether), making the data accessible by a variety of criteria. Thus, chemists can use the dictionary to find information on how to analyze for a particular substance, how a particular compound may be used as an analytical reagent or what other reagents are available for a specific analytical use. Having located all appropriate reagents via the index, the user can then browse through the entries to obtain specific data, all fully referenced in the selective bibliography. Analytical chemists - be they in the manufacturing or pharmaceutical industry, working in hospital laboratories as clinical chemists or pollution analysts monitoring heavy metal residues in waste water - constantly need to make decisions about which reagent to choose for a particular application. This dictionary fulfils that need by being the most comprehensive, reliable and up-to-date compilation of reagents available. This book should be of interest to analytical chemists in academic and industrial establishments, forensic scientists, chromatographers, biochemists, standards institutions, companies selling laboratory chemicals, and water authorities.