Physico Chemical Applications Of Nmr

Author : A. B. Kudryavtsev
Publisher : World Scientific
ISBN 13 : 9789810225407
Total Pages : 380 pages
Book Rating : 4.07/5 ( download)

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Download or read book Physico-chemical Applications of NMR written by A. B. Kudryavtsev and published by World Scientific. This book was released on 1996 with total page 380 pages. Available in PDF, EPUB and Kindle. Book excerpt: The book is intended to help under- and postgraduate students and young scientists in the correct application of NMR to the solution of physico-chemical problems concerning the study of equilibria in solution. The first part of the book (Chapters 1-3) is a trivium, but should enable a student to design and conduct simple physico-chemical NMR experiments. The following chapters give illustrative material on the physico-chemical applications of NMR of increasing complexity. These chapters include the problem of determination of equilibrium and rate constants in solution, the study of paramagnetism using NMR, the application of Dynamic NMR techniques and relaxation measurements. A multipurpose nonlinear regression program is supplied (on disc for PC) and is referred to throughout the book.

Author : Klaus Müller
Publisher : John Wiley & Sons
ISBN 13 : 3527690115
Total Pages : 560 pages
Book Rating : 4.14/5 ( download)

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Download or read book Solid State NMR written by Klaus Müller and published by John Wiley & Sons. This book was released on 2021-06-23 with total page 560 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid State NMR A thorough and comprehensive textbook covering the theoretical background, experimental approaches, and major applications of solid-state NMR spectroscopy Nuclear Magnetic Resonance (NMR) spectroscopy is a powerful non-destructive technique capable of providing information about the molecular structure and dynamics of molecules. Alongside solution-state NMR, a well-established technique to study chemical structures and investigate physico-chemical properties of molecules in solutions, solid-state NMR (SSNMR) offers many exciting possibilities for the analysis of solid and soft materials across scientific fields. SSNMR shows unique capabilities for a detailed investigation of structural and dynamic properties of materials over wide space and time ranges. For this reason, and thanks to significant advances in the past several years, the application of SSNMR to materials is rapidly increasing in disciplines such as chemistry, physics, and materials and life sciences. Solid State NMR: Principles, Methods, and Applications offers a systematic introduction to the theory, methodological concepts, and major experimental methods of SSMR spectroscopy. Exploring the unique potential of SSNMR for the structural and dynamic characterization of soft and either amorphous or crystalline solid materials, this comprehensive textbook provides foundational knowledge and recent developments of SSNMR, covering physical and theoretical background, experimental methods, and applications to pharmaceuticals, polymers, inorganic and hybrid materials, liquid crystals, and model membranes. Written by two expert authors to ensure a clear and consistent presentation of the subject, this textbook: Includes a brief introduction to the historical aspects and broad theoretical background of solid-state NMR spectroscopy Provides helpful illustrations to explain the various SSNMR concepts and methods Features accessible descriptive text with self-consistent use of quantum mechanics Covers the experimental aspects of SSNMR spectroscopy and in particular a description of many useful pulse sequences Contains references to relevant literature Solid State NMR: Principles, Methods, and Applications is the ideal textbook for university courses on SSNMR, advanced spectroscopies, and a valuable single-volume reference for spectroscopists, chemists, and researchers in the field of materials.

Author : B. Lindman
Publisher : Springer Science & Business Media
ISBN 13 : 364266363X
Total Pages : 381 pages
Book Rating : 4.35/5 ( download)

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Download or read book Chlorine, Bromine and Iodine NMR written by B. Lindman and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 381 pages. Available in PDF, EPUB and Kindle. Book excerpt: The increasing interest in NMR spectroscopy of what in some confer ences in this field is commonly termed "other nuclei" is unmistakable. Chemists and biologists who employ NMR spectroscopy to study their problems have, however, been somewhat reluctant to study nuclei with electric quadrupole moments. These nuclei frequently give rise to broad NMR signals, sometimes too broad to be detectable with ordinary high resolution NMR spectrometers. Spectrometers that could cope with broad NMR signals of low intensity, "wide-line" spectrometers, have been available since the mid 1950:s but it appears that most of these instruments ended up in physical laboratories where the research was primarily directed towards solid state problems. The study of quadrupolar nuclei can provide unique and very valuable information on a variety of physico-chemical and biological systems. For one thing the relaxation of quadrupolar nuclei is in many ways easier to interpret than the relaxation of non-quadrupolar nuclei, since the former is in many cases caused by purely intramolecular interactions modulated by the molecular motion. Studies of quadrupolar relaxation have therefore furnished important information about molec ular reorientation and association in liquids and have played - and will certainly play for many years - an important role in testing new theoretical models of molecular motion in liquids.

Author : Oliver Zerbe
Publisher : John Wiley & Sons
ISBN 13 : 3527677836
Total Pages : 581 pages
Book Rating : 4.32/5 ( download)

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Download or read book Applied NMR Spectroscopy for Chemists and Life Scientists written by Oliver Zerbe and published by John Wiley & Sons. This book was released on 2013-11-26 with total page 581 pages. Available in PDF, EPUB and Kindle. Book excerpt: From complex structure elucidation to biomolecular interactions - this applicationoriented textbook covers both theory and practice of modern NMR applications. Part one sets the stage with a general description of NMR introducing important parameters such as the chemical shift and scalar or dipolar couplings. Part two describes the theory behind NMR, providing a profound understanding of the involved spin physics, deliberately kept shorter than in other NMR textbooks, and without a rigorous mathematical treatment of all the physico-chemical computations. Part three discusses technical and practical aspects of how to use NMR. Important phenomena such as relaxation, exchange, or the nuclear Overhauser effects and the methods of modern NMR spectroscopy including multidimensional experiments, solid state NMR, and the measurement of molecular interactions are the subject of part four. The final part explains the use of NMR for the structure determination of selected classes of complex biomolecules, from steroids to peptides or proteins, nucleic acids, and carbohydrates. For chemists as well as users of NMR technology in the biological sciences.

Author : B. I. Ionin
Publisher : Springer Science & Business Media
ISBN 13 : 1468417851
Total Pages : 396 pages
Book Rating : 4.52/5 ( download)

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Download or read book NMR Spectroscopy in Organic Chemistry written by B. I. Ionin and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 396 pages. Available in PDF, EPUB and Kindle. Book excerpt: In recent years high-resolution nuclear magnetic resonance spec troscopy has found very wide application in organie chemistry in structural and physicochemical investigations and. also in the study of the characteristics of organic compounds which are re lated to the distribution of the electron cloud in the molecules. The vigorous development of this method, which may really be re garded as an independent branch of science, is the result of ex tensive progress in NMR technology, the refinement of its theory, and the accumulation of large amounts of experimental material, which has been correlated by empiricallaws and principles. The literature directly concerned with the NMR method and its applica tion has now grown to such an extent that a complete review of it is practically impossible. Therefore the authors have limited themselves to an examination of only the most important, funda mental, and general investigations. The book consists of six chapters. In the first chapter we have attempted to present the fundamentals of the NMR method in such a way that the reader with little knowledge of the subject will be able to use the method in practical work for investigating simple compounds and solving simple problems. The three subsequent chapters give a deeper analysis of the method, while the last two chapters and the appendix illustrate the various applications of NMR spectroscopy in organic chemistry.

Author : Thomas C. Pochapsky
Publisher :
ISBN 13 : 9780203833490
Total Pages : pages
Book Rating : 4.9X/5 ( download)

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Download or read book NMR for Physical and Biological Scientists written by Thomas C. Pochapsky and published by . This book was released on 2006 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: "Nuclear Magnetic Resonance spectroscopy is a dynamic way for scientists of all kinds to investigate the physical, chemical, and biological properties of matter.Its many applications make it a versatile tool previously subject to monolithic treatment in reference-style texts. Based on a course taught for over ten years at Brandeis University, this is the first textbook on NMR spectroscopy for a one-semester course or self-instruction. In keeping with the authors' efforts to make it a useful textbook, they have included problems at the end of each chapter.The book not only covers the latest developments in the field, such as GOESY (Gradient Enhanced Overhauser Spectroscopy) and multidimensional NMR, but includes practical examples using real spectra and associated problem sets. Assuming the reader has a background of chemistry, physics and calculus, this textbook will be ideal for graduate students in chemistry and biochemistry, as well as biology, physics, and biophysics.NMR for Physical and Biological Scientists will also be useful to medical schools, research facilities, and the many chemical, pharmaceutical, and biotech firms that offer in-house instruction on NMR spectroscopy."--Provided by publisher.

Author : Edwin D. Becker
Publisher : Elsevier
ISBN 13 : 148326789X
Total Pages : 325 pages
Book Rating : 4.90/5 ( download)

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Download or read book High Resolution NMR written by Edwin D. Becker and published by Elsevier. This book was released on 2013-10-22 with total page 325 pages. Available in PDF, EPUB and Kindle. Book excerpt: High Resolution NMR: Theory and Chemical Applications focuses on the applications of nuclear magnetic resonance (NMR), as well as chemical shifts, lattices, and couplings. The book first offers information on the theory of NMR, including nuclear spin and magnetic moment, spin lattice relaxation, line widths, saturation, quantum mechanical description of NMR, and ringing. The text then ponders on instrumentation and techniques and chemical shifts. Discussions focus on the origin of chemical shifts, reference compounds, empirical correlations of chemical shifts, modulation and phase detection, requirements for high resolution NMR, and superconducting magnets. The text elaborates on electron-coupled spin-spin interactions, as well as origin of spin-spin coupling, signs of coupling constants, theory of spin-spin coupling, correlation of coupling constants with other physical properties, and observed coupling constant. The manuscript also ponders on the use of NMR in structure elucidation, theory and applications of double resonance, and analysis of complex spectra. The publication is a dependable reference for readers interested in high resolution NMR.

Author : A B Kudryavtsev
Publisher : World Scientific
ISBN 13 : 9814499455
Total Pages : 372 pages
Book Rating : 4.53/5 ( download)

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Download or read book Physico-Chemical Applications of NMR written by A B Kudryavtsev and published by World Scientific. This book was released on 1996-09-20 with total page 372 pages. Available in PDF, EPUB and Kindle. Book excerpt: The book is intended to help under- and postgraduate students and young scientists in the correct application of NMR to the solution of physico-chemical problems concerning the study of equilibria in solution. The first part of the book (Chapters 1–3) is a trivium, but should enable a student to design and conduct simple physico-chemical NMR experiments. The following chapters give illustrative material on the physico-chemical applications of NMR of increasing complexity. These chapters include the problem of determination of equilibrium and rate constants in solution, the study of paramagnetism using NMR, the application of Dynamic NMR techniques and relaxation measurements. A multipurpose nonlinear regression program is supplied (on disc for PC) and is referred to throughout the book. Contents: NMR — Basic PrinciplesExperimental Techniques Employed in NMRThe Analysis of Experimental Data by Regression TechniquesStudies of Equilibria in the Liquid State by NMR SpectroscopyStudies of Paramagnetism in Solutions by NMRDynamic NMR and Nuclear Magnetic Relaxation MeasurementsAppendicesAddendum: Encounter with NMR Instruments Readership: Students and researchers in analytical chemistry, inorganic chemistry and physical chemistry. keywords:NMR Spectroscopy;Practical FT NMR;Regression Methods;NMR Relaxation;Dynamic NMR;NMR of Paramagnetics;Physical Chemistry;Chemical Equilibrium;Chemical Kinetics;Solutions;Cements

Author : Robin Kingsley Harris
Publisher : Prentice Hall
ISBN 13 :
Total Pages : 288 pages
Book Rating : 4.21/5 ( download)

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Download or read book Nuclear Magnetic Resonance Spectroscopy written by Robin Kingsley Harris and published by Prentice Hall. This book was released on 1986 with total page 288 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nuclear Magnetic Resonance Spectroscopy explains the NMR phenomenon from the point of view of a physical chemist interested in both fundamental principles and chemical applications. This rigorous but lucid text is highlighted by a large number of figures including illustrative spectra. Problems - with answers where appropriate - are also included. Table of contents: 1: The fundamentals; 2: Analysis of NMR spectra for isotropic solutions; 3: Relaxation and Fourier transform NMR; 4: Dipolar interactions and double resonance; 5: Chemical exchange and quadrupolar effects; 6: NMR of the solid state; 7: Special pulse sequences and two-dimensional NMR; 8: Chemical shifts and coupling constants. Appendices. Further reading. Answers to problems. Index.

Author : Norman S. Bhacca
Publisher :
ISBN 13 :
Total Pages : 216 pages
Book Rating : 4.82/5 ( download)

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Download or read book Applications of NMR Spectroscopy in Organic Chemistry written by Norman S. Bhacca and published by . This book was released on 1964 with total page 216 pages. Available in PDF, EPUB and Kindle. Book excerpt: