Characterization Of Porous Solids

Author : S. Lowell
Publisher : Springer Science & Business Media
ISBN 13 : 1402023030
Total Pages : 365 pages
Book Rating : 4.33/5 ( download)

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Download or read book Characterization of Porous Solids and Powders: Surface Area, Pore Size and Density written by S. Lowell and published by Springer Science & Business Media. This book was released on 2012-09-14 with total page 365 pages. Available in PDF, EPUB and Kindle. Book excerpt: The growth of interest in newly developed porous materials has prompted the writing of this book for those who have the need to make meaningful measurements without the benefit of years of experience. One might consider this new book as the 4th edition of "Powder Surface Area and Porosity" (Lowell & Shields), but for this new edition we set out to incorporate recent developments in the understanding of fluids in many types of porous materials, not just powders. Based on this, we felt that it would be prudent to change the title to "Characterization of Porous Solids and Powders: Surface Area, Porosity and Density". This book gives a unique overview of principles associated with the characterization of solids with regard to their surface area, pore size, pore volume and density. It covers methods based on gas adsorption (both physi and chemisorption), mercury porosimetry and pycnometry. Not only are the theoretical and experimental basics of these techniques presented in detail but also, in light of the tremendous progress made in recent years in materials science and nanotechnology, the most recent developments are described. In particular, the application of classical theories and methods for pore size analysis are contrasted with the most advanced microscopic theories based on statistical mechanics (e.g. Density Functional Theory and Molecular Simulation). The characterization of heterogeneous catalysts is more prominent than in earlier editions; the sections on mercury porosimetry and particularly chemisorption have been updated and greatly expanded.

Author : H. Kral
Publisher : Elsevier
ISBN 13 : 9780080960739
Total Pages : 644 pages
Book Rating : 4.31/5 ( download)

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Download or read book Characterization of Porous Solids written by H. Kral and published by Elsevier. This book was released on 1988-04-01 with total page 644 pages. Available in PDF, EPUB and Kindle. Book excerpt: The importance of porosity has long been recognized by scientists and engineers. Porous solids are widely encountered in industry and everyday life and their behaviour, e.g. chemical reactivity, adsorptive capacity, and catalytic activity is dependent on their pore structure. A considerable amount of work on porous solids has been undertaken both in academic and in industrial laboratories. However, all this activity is in urgent need of a critical appraisal. To undertake this task, a number of leading experts in the field of adsorption, porosimetry, X-ray and neutron scattering, optical and electron microscopy, calorimetry and fluid permeation, were brought together at the 1987 IUPAC (COPS I) Symposium. This proceedings volume provides an up-to-date overall review of the theoretical foundations for modelling and characterizing porous systems. It deals with most of the techniques in current use as applied to both model systems and porous solids of industrial importance. The reader will find the description and discussion of a number of novel techniques as well as a critical appraisal and comparison of the more established methods. All those concerned with the characterization of porous solids in academic and industrial laboratories will find much to interest them in this volume. It should be on the bookshelf of applied research centres involved in adsorption, catalysis, purification of gases and liquids, pigments, fillers, building materials, etc.

Author : Seymour Lowell
Publisher : Springer Science & Business Media
ISBN 13 : 9781402023026
Total Pages : 370 pages
Book Rating : 4.22/5 ( download)

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Download or read book Characterization of Porous Solids and Powders: Surface Area, Pore Size and Density written by Seymour Lowell and published by Springer Science & Business Media. This book was released on 2006-04-24 with total page 370 pages. Available in PDF, EPUB and Kindle. Book excerpt: The growth of interest in newly developed porous materials has prompted the writing of this book for those who have the need to make meaningful measurements without the benefit of years of experience. One might consider this new book as the 4th edition of "Powder Surface Area and Porosity" (Lowell & Shields), but for this new edition we set out to incorporate recent developments in the understanding of fluids in many types of porous materials, not just powders. Based on this, we felt that it would be prudent to change the title to "Characterization of Porous Solids and Powders: Surface Area, Porosity and Density". This book gives a unique overview of principles associated with the characterization of solids with regard to their surface area, pore size, pore volume and density. It covers methods based on gas adsorption (both physi and chemisorption), mercury porosimetry and pycnometry. Not only are the theoretical and experimental basics of these techniques presented in detail but also, in light of the tremendous progress made in recent years in materials science and nanotechnology, the most recent developments are described. In particular, the application of classical theories and methods for pore size analysis are contrasted with the most advanced microscopic theories based on statistical mechanics (e.g. Density Functional Theory and Molecular Simulation). The characterization of heterogeneous catalysts is more prominent than in earlier editions; the sections on mercury porosimetry and particularly chemisorption have been updated and greatly expanded.

Author : G. Kreysa
Publisher : Elsevier
ISBN 13 : 0080528899
Total Pages : 699 pages
Book Rating : 4.92/5 ( download)

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Download or read book Characterisation of Porous Solids V written by G. Kreysa and published by Elsevier. This book was released on 2000-04-11 with total page 699 pages. Available in PDF, EPUB and Kindle. Book excerpt: The Fifth International Symposium on the Characterisation of Porous Solids (COPS-V) was held at Heidelberg, Germany, from May 30 to June 2, 1999. About 220 participants from 25 countries enjoyed a very successful meeting with 32 lectures and 155 poster presentations. The Symposium started with a highly stimulating lecture by Sir John Meurig Thomas, Cambridge, highlighting the recent developments in engineering of new catalysts. The following two full sessions were devoted to theory, modelling and simulation which provide the basis for the interpretation of pore structural data of adsorbents and finely dispersed solids. Sessions 2 and 3 focused on the advances in the synthesis and characterisation of highly ordered inorganic adsorbents and carbons. Sessions 4 and 5 addressed important questions with respect to the characterisation of porous solids by sorption measurement and other related techniques. The intensive three-day programme provided a stimulating forum for the exchange of novel research findings, concepts, techniques and materials which are collected in this volume.

Author :
Publisher : Elsevier
ISBN 13 : 0080528910
Total Pages : 809 pages
Book Rating : 4.15/5 ( download)

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Download or read book Characterization of Porous Solids VI written by and published by Elsevier. This book was released on 2002-11-14 with total page 809 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book contains 99 of the papers that were presented at the 6th in the series of Symposia on Characterization of Porous Solids held in Alicante, Spain, May 2002. Written by leading international specialists in the subject, the contributions represent an up-to-date and authoritative account of recent developments around the world in the major methods used to characterize porous solids. The book is a useful work of reference for anyone interested in characterizing porous solids, such as MCM-41 mesoporous materials, pillared clays, etc. Papers on pore structure determination using gas adsorption feature strongly, together with papers on small angle scattering methods, mercury porosimetry, microcalorimetry, scanning probe microscopies, and image analysis.

Author : Valentin Valtchev
Publisher : Elsevier
ISBN 13 : 9780080932453
Total Pages : 800 pages
Book Rating : 4.52/5 ( download)

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Download or read book Ordered Porous Solids written by Valentin Valtchev and published by Elsevier. This book was released on 2011-08-11 with total page 800 pages. Available in PDF, EPUB and Kindle. Book excerpt: The developments in the area of ordered nanoporous solids have moved beyond the traditional catalytic and separation uses and given rise to a wide variety of new applications in different branches of chemistry, physics, material science, etc. The activity in this area is due to the outstanding properties of nanoporous materials that have attracted the attention of researchers from different communities. However, recent achievements in a specific field often remain out of the focus of collaborating communities. This work summarizes the latest developments and prospects in the area of ordered porous solids, including synthetic layered materials (clays), microporous zeolite-type materials, ordered mesoporous solids, metal-organic-framework compounds (MOFs), carbon, etc. All aspects, from synthesis via comprehensive characterization to the advanced applications of ordered porous materials, are presented. The chapters are written by leading experts in their respective fields with an emphasis on recent progress and the state of the art. * Summarizes the latest developments in the field of ordered nanoporous solids * Presents state-of-the-art coverage of applications related to porous solids * Incorporates 28 contributions from experts across the disciplines

Author : Jean Rouquerol
Publisher : Academic Press
ISBN 13 : 0080970362
Total Pages : 647 pages
Book Rating : 4.63/5 ( download)

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Download or read book Adsorption by Powders and Porous Solids written by Jean Rouquerol and published by Academic Press. This book was released on 2013-09-06 with total page 647 pages. Available in PDF, EPUB and Kindle. Book excerpt: The declared objective of this book is to provide an introductory review of the various theoretical and practical aspects of adsorption by powders and porous solids with particular reference to materials of technological importance. The primary aim is to meet the needs of students and non-specialists who are new to surface science or who wish to use the advanced techniques now available for the determination of surface area, pore size and surface characterization. In addition, a critical account is given of recent work on the adsorptive properties of activated carbons, oxides, clays and zeolites. Provides a comprehensive treatment of adsorption at both the gas/solid interface and the liquid/solid interface Includes chapters dealing with experimental methodology and the interpretation of adsorption data obtained with porous oxides, carbons and zeolites Techniques capture the importance of heterogeneous catalysis, chemical engineering and the production of pigments, cements, agrochemicals, and pharmaceuticals

Author :
Publisher :
ISBN 13 : 9780444418012
Total Pages : 645 pages
Book Rating : 4.16/5 ( download)

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Download or read book Characterization of Porous Solids written by and published by . This book was released on 1988 with total page 645 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Author : Pascal Van Der Voort
Publisher : John Wiley & Sons
ISBN 13 : 111942660X
Total Pages : 441 pages
Book Rating : 4.08/5 ( download)

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Download or read book Introduction to Porous Materials written by Pascal Van Der Voort and published by John Wiley & Sons. This book was released on 2019-08-19 with total page 441 pages. Available in PDF, EPUB and Kindle. Book excerpt: The first comprehensive textbook on the timely and rapidly developing topic of inorganic porous materials This is the first textbook to completely cover a broad range of inorganic porous materials. It introduces the reader to the development of functional porous inorganic materials, from the synthetic zeolites in the 50’s, to today’s hybrid materials such as metal-organic frameworks (MOFs), covalent organic frameworks (COFs) and related networks. It also provides the necessary background to understand how porous materials are organized, characterized, and applied in adsorption, catalysis, and many other domains. Additionally, the book explains characterization and application from the materials scientist viewpoint, giving the reader a practical approach on the characterization and application of the respective materials. Introduction to Inorganic Porous Materials begins by describing the basic concepts of porosity and the different types of pores, surfaces, and amorphous versus crystalline materials, before introducing readers to nature’s porous materials. It then goes on to cover everything from adsorption and catalysis to amorphous materials such as silica to inorganic carbons and Periodic Mesoporous Organosilicas (PMOs). It discusses the synthesis and applications of MOFs and the broad family of COFs. It concludes with a look at future prospects and emerging trends in the field. The only complete book of its kind to cover the wide variety of inorganic and hybrid porous materials A comprehensive reference and outstanding tool for any course on inorganic porous materials, heterogeneous catalysis, and adsorption Gives students and investigators the opportunity to learn about porous materials, how to characterize them, and understand how they can be applied in different fields Introduction to Inorganic Porous Materials is an excellent book for students and professionals of inorganic chemistry and materials science with an interest in porous materials, functional inorganic materials, heterogeneous catalysis and adsorption, and solid state characterization techniques.

Author : Andrei S. Dukhin
Publisher : Elsevier
ISBN 13 : 0444639071
Total Pages : 590 pages
Book Rating : 4.73/5 ( download)

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Download or read book Characterization of Liquids, Dispersions, Emulsions, and Porous Materials Using Ultrasound written by Andrei S. Dukhin and published by Elsevier. This book was released on 2017-08-08 with total page 590 pages. Available in PDF, EPUB and Kindle. Book excerpt: Characterization of Liquids, Dispersions, Emulsions and Porous Materials Using Ultrasound, Third Edition, presents a scientific background for novel methods of characterizing homogeneous and heterogeneous liquids (dispersions, emulsions, and gels) as well as porous materials. Homogeneous liquids are characterized in rheological terms, whereas particle-size distribution and zeta potential are parameters of heterogeneous liquids. For porous materials, porosity, pore size, and zeta potential are output characteristics. These methods are based on ultrasound, which opens an opportunity for simplifying the sample preparation by eliminating dilution. This in turn, makes measurements faster, easier, precise, suitable for accurate quality control, PAT, and formulation of complex systems. This book provides theoretical background of acoustics, rheology, colloid science, electrochemistry, and other relevant scientific fields, describing principles of existing instrumentation and, in particular, commercially available instruments. Finally, the book features an extensive list of existing applications. Presents a theoretical multi-disciplinary background of several new ultrasound analytical techniques in one place Validates the theoretical basis of several new analytical techniques Compares the efficiency and applications of various ultrasound techniques Lists many ultrasound applications in colloid chemistry Contains an extensive bibliography on this multidisciplinary topic